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Question
1.95 gm of coal sample was taken for nitrogen estimation by Kjeldahl’s method. The ammonia liberated required 9.5 ml of 0.4 N H2SO4 for neutralization. Calculate the percentage of nitrogen in coal sample.
Numerical
Solution
Given:
Weight Of Coal= 1.95 gm Normality of H2SO4= 0.4 N
Volume of H2SO4= 9.5 ml
Required: % N=?
Formula: %N=`("vol of" H_2SO^4xx"Normality"xx1.4)/"wt of coal"`
%N= `(9.5xx0.4xx1.4)/(1.95)`
%N= 2.72%
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Solid Fuels - Analysis of Coal
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